Intangiriro ku miyoboro mito ya Peptide Trace Mineral Chelates
Igice cya 1 Amateka y'inyongeramusaruro z'amabuye y'agaciro
Ishobora kugabanywamo ibisekuru bine hakurikijwe iterambere ry’inyongeramusaruro z’imyunyu ngugu:
Igisata cya mbere: Umunyu w’imyunyu ngugu utari uw’umwimerere, nka sulfate y’umuringa, sulfate y’umuringa, okiside ya zinki, nibindi; Igisata cya kabiri: Umunyu w’imyunyu ngugu utari uw’umwimerere, nka lactate y’umuringa, fumarate y’umuringa, citrate y’umuringa, nibindi; Igisata cya gatatu: Ingano y’imyunyu ngugu ya aside chelate y’imyunyu ngugu utari uw’umwimerere, nka methionine ya zinki, glycine y’icyuma na glycine ya zinki; Igisata cya kane: Umunyu wa poroteyine n’imyunyu ngugu ya peptide chelating y’imyunyu ngugu utari uw’umwimerere, nka poroteyine y’umuringa, poroteyine y’icyuma, poroteyine y’icyuma, poroteyine y’icyuma, manganese y’icyuma, peptide ntoya y’umuringa, peptide ntoya y’icyuma, peptide ntoya y’icyuma, manganese y’icyuma, nibindi.
Igisata cya mbere ni imyunyu ngugu idakomoka ku binyabuzima, naho igisata cya kabiri kugeza ku cya kane ni imyunyu ngugu idakomoka ku binyabuzima.
Igice cya 2 Impamvu yo Guhitamo Chelate nto za Peptide
Chelate nto ya peptide ifite akamaro gakurikira:
1. Iyo peptide nto zivanze na iyoni z'icyuma, ziba zikungahaye ku miterere kandi bigora kuzishyiramo;
2. Ntabwo ihangana n'imiyoboro ya aside amine, ifite ahantu henshi ho kwinjiza kandi yihuta mu kwinjiza;
3. Gukoresha ingufu nke; 4. Amafaranga menshi abikwa, uburyo bwo gukoresha amatungo menshi kandi umusaruro wayo urushaho kuba mwiza cyane;
5. Irwanya bagiteri n'irwanya ogisijeni;
6. Kugenga ubudahangarwa bw'umubiri.
Ubushakashatsi bwinshi bwagaragaje ko imiterere cyangwa ingaruka za peptide chelate ntoya zituma zigira amahirwe menshi yo gukoreshwa no guteza imbere, bityo ikigo cyacu cyafashe icyemezo cyo gufata peptide chelate ntoya nk'ikintu cy'ingenzi mu bushakashatsi no guteza imbere ibikomoka ku mabuye y'agaciro y’ingirabuzimafatizo y’ikigo.
Igice cya 3 Ingufu za peptide chelate nto
1. Isano iri hagati ya peptide, aside amine na poroteyine
Uburemere bwa molekile ya poroteyine burenga 10000;
Uburemere bwa molekile ya peptide ni 150 ~ 10000;
Peptide nto, zitwa kandi peptide ntoya za molekile, zigizwe na aside amine 2 ~ 4;
Uburemere bw'ingirabuzimafatizo za aside amine ni hafi 150.
2. Guhuza amatsinda ya aside amine na peptides chelated hamwe n'ibyuma
(1) Amatsinda ahuza aside amine
Amatsinda ahuza aside amine:
Amatsinda ya amino na karuboni kuri a-karuboni;
Amatsinda y’uruhererekane rw’aside amine zimwe na zimwe, nka sulfhydryl itsinda rya cysteine, phenolic itsinda rya tyrosine na imidazole itsinda rya histidine.
(2) Guhuza amatsinda muri peptides nto
Peptide nto zifite amatsinda menshi ahuza ibintu kurusha aside amine. Iyo zivanze n'iyoni z'icyuma, biroroha kuzihuza, kandi zishobora gukora ubwiyongere bw'amanota menshi, bigatuma ubwiyongere bukomera.
3. Ingufu z'umusaruro muto wa peptide chelate
Ishingiro ry'inyigisho za peptide ntoya zituma imyunyu ngugu ifata neza
Imiterere y’uburyo peptide nto zifata ni yo shingiro ry’inyigisho zo guteza imbere uburyo ibintu bito bifatwa nk’ibice by’ingenzi byinjizwamo. Dukurikije inyigisho gakondo ya poroteyine, icyo inyamaswa zikenera kuri poroteyine ni icyo zikenera kuri aside amine zitandukanye. Ariko, mu myaka ya vuba aha, ubushakashatsi bwagaragaje ko igipimo cy’ikoreshwa rya aside amine mu biryo biva ahantu hatandukanye gitandukanye, kandi iyo inyamaswa zigaburirwa indyo ya homozygous cyangwa indyo ifite aside amine nkeya ya poroteyine, umusaruro mwiza ntushobora kuboneka (Baker, 1977; Pinchasov et al., 1990) [2,3]. Kubwibyo, bamwe mu bahanga batanze igitekerezo cy’uko inyamaswa zifite ubushobozi bwihariye bwo gufata poroteyine ubwayo cyangwa peptide zifitanye isano. Agar (1953) [4] yabanje kubona ko inzira y’amara ishobora gufata no gutwara diglycidyl burundu. Kuva icyo gihe, abashakashatsi batanze impamvu yemeza ko peptide nto zishobora kwinjiramo burundu, zemeza ko glycylglycine ikora itwarwa kandi ikanashyirwamo; Umubare munini wa peptide nto zishobora kwinjira mu buryo butaziguye mu miyoboro y’amaraso mu buryo bwa peptide. Hara et al. (1984)[5] yanagaragaje ko umusaruro wa poroteyine mu gifu mu nzira y’igifu ahanini ari peptide ntoya aho kuba aside amine zigenga (FAA). Peptide nto zishobora kunyura mu turemangingo tw’amara neza no kwinjira mu miyoboro y’amaraso (Le Guowei, 1996)[6].
Iterambere ry'ubushakashatsi ku bijyanye na Peptide ntoya itera imbaraga mu kwinjiza amabuye y'agaciro, Qiao Wei, n'abandi.
Peptide ntoya zitwarwa kandi zigashyirwa mu buryo bwa peptide ntoya
Dukurikije uburyo bwo kwinjiza no gutwara hamwe n'imiterere ya peptide nto, imyunyu ngugu ihuza na peptide nto kuko ligande nkuru zishobora gutwarwa zose hamwe, ibyo bikaba byiza cyane mu kunoza imbaraga za biyoloji z'imyunyu ngugu. (Qiao Wei, et al)
Ingufu za Chelate nto za Peptide
1. Iyo peptide nto zivanze na iyoni z'icyuma, ziba zikungahaye ku miterere kandi bigora kuzishyiramo;
2. Ntabwo ihangana n'imiyoboro ya aside amine, ifite ahantu henshi ho kwinjiza kandi yihuta mu kwinjiza;
3. Ingufu nke zikoreshwa;
4. Amafaranga menshi yo kubitsa, igipimo cyo gukoresha cyane no kunoza umusaruro w'amatungo;
5. Irwanya bagiteri n'irwanya ogisijeni; 6. Kugenzura ubudahangarwa bw'umubiri.
4. Gusobanukirwa byimbitse peptides
Ni nde muri aba bantu babiri bakoresha peptide uhabwa amahirwe menshi?
- Peptide ihuza
- Fosfopeptide
- Ibikoresho bifitanye isano
- Peptide irwanya mikorobe
- Peptide y'ubudahangarwa bw'umubiri
- Neuropeptide
- Peptide y'imisemburo
- Peptide irwanya ogisijeni
- Peptide z'imirire
- Peptide zitera ibirungo
(1) Gushyira mu byiciro peptides
(2) Ingaruka za peptides ku miterere y'umubiri
- 1. Guhindura uburinganire bw'amazi n'amashanyarazi mu mubiri;
- 2. Gukora ubudahangarwa bw'umubiri burwanya bagiteri n'indwara kugira ngo ubudahangarwa bw'umubiri burusheho gukora neza;
- 3. Gufasha gukira kw'ibikomere; Gusana vuba ibikomere byo mu ruhu.
- 4. Gukora imisemburo mu mubiri bifasha guhindura ibiryo mo ingufu;
- 5. Gusana uturemangingo, kunoza imikorere y'uturemangingo, gukumira kwangirika kw'uturemangingo, no kugira uruhare mu gukumira kanseri;
- 6. Guteza imbere imikorere n'imikorere ya poroteyine na enzymes;
- 7. Ubutumwa bw'ingenzi bw'ibinyabutabire bwo gutumanaho amakuru hagati y'uturemangingo n'ingingo;
- 8. Kwirinda indwara z'umutima n'imitsi yo mu bwonko;
- 9. Kugenzura imisemburo y'amaraso n'imitsi.
- 10. Kunoza uburyo bwo kugogora no kuvura indwara zidakira z’igifu;
- 11. Kunoza indwara za diyabete, rubagimpande, rubagimpande n'izindi.
- 12. Kurwanya kwandura virusi, kurwanya gusaza, gukuraho uturemangingo twinshi tw’umubiri.
- 13. Guteza imbere imikorere y'amaraso, kuvura amaraso make, gukumira kwibumbira kwa platelet, bishobora kongera ubushobozi bw'uturemangingo dutukura tw'amaraso gutwara ogisijeni.
- 14. Kurwanya virusi za ADN mu buryo butaziguye no kwibasira bagiteri za virusi.
5. Imikorere ibiri y'imirire ya chelate nto za peptide
Peptide chelate ntoya yinjira mu ngirabuzimafatizo yose mu mubiri w'inyamaswa, mazehanyuma bigahita bikuraho umugozi wa chelationmu ngirabuzimafatizo maze ikaranduka mo iyoni za peptide na metal, zikoreshwa nainyamaswa kugira ngo igire imirimo ibiri mu mirirecyane cyaneuruhare rw'imikorere ya peptide.
Imikorere ya peptide nto
- 1. Guteza imbere poroteyine mu mitsi y'inyamaswa, kugabanya apoptosis, no guteza imbere imikurire y'inyamaswa
- 2. Kunoza imiterere y'ibimera byo mu mara no guteza imbere ubuzima bw'amara
- 3. Gutanga amagufwa ya karuboni no kongera imikorere ya enzymes zo mu gifu nka amylase y'amara na poroteyine
- 4. Bigira ingaruka ku muvuduko wo kurwanya ogisijeni
- 5. Afite ubushobozi bwo kurwanya ububyimbirwe
- 6.……
6. Ibyiza bya chelate nto za peptide kuruta chelate za aside amine
| Imyunyu ngugu ya aside amine ikomoka kuri aside amine | Imyunyu ngugu mito ya peptide chelated trace | |
| Igiciro cy'ibikoresho fatizo | Ibikoresho fatizo bya aside amine imwe birahenze | Ibikoresho fatizo bya keratin byo mu Bushinwa biraboneka cyane. Umusatsi, ibinono n'amahembe mu bworozi bw'amatungo ndetse n'ibisigazwa by'amazi mabi ya poroteyine n'ibisigazwa by'uruhu mu nganda z'imiti ni ibikoresho fatizo bya poroteyine byiza kandi bihendutse. |
| Ingaruka zo kwinjiza | Amatsinda ya amino na karubokisili agira uruhare icyarimwe mu gutandukanya aside amino n'ibintu by'icyuma, bigakora imiterere ya bicyclic endocannabinoid isa n'iya dipeptides, nta matsinda ya karubokisili y'ubuntu ahari, ashobora kwinjizwa gusa binyuze muri sisitemu ya oligopeptide. (Su Chunyang et al., 2002) | Iyo peptide nto zigize uruhare muri chelation, imiterere ya chelation imwe muri rusange ikorwa n'itsinda rya amino rigizwe n'agace ka terminal na ogisijeni ya peptide ifatanye, kandi chelate igumana itsinda rya karboksili ryigenga, rishobora kwinjiza binyuze muri sisitemu ya dipeptide, rifite imbaraga zo kwinjiza nyinshi kurusha sisitemu ya oligopeptide. |
| Ituze | Iyoni z'icyuma zifite impeta imwe cyangwa nyinshi zifite ibice bitanu cyangwa bitandatu by'amatsinda ya amino, amatsinda ya karubokisili, amatsinda ya imidazoli, amatsinda ya phenoli, na sulfhydryl. | Uretse amatsinda atanu asanzweho ya aside amine, amatsinda ya karuboni na imino muri peptide ntoya nabyo bishobora kugira uruhare mu guhuza, bityo bigatuma chelate nto za peptide zihamye kurusha chelate za aside amine. (Yang Pin et al., 2002) |
7. Ibyiza bya chelate nto za peptide kuruta aside glycolic na chelate za methionine
| Imyunyu ngugu ya Glycine chelated | Imyunyu ngugu ya methionine chelated | Imyunyu ngugu mito ya peptide chelated trace | |
| Ifishi yo guhuza ibikorwa | Amatsinda ya karboksili na amino ya glycine ashobora guhuzwa na iyoni z'icyuma. | Amatsinda ya karubokisili n'amino ya methionine ashobora guhuzwa na iyoni z'icyuma. | Iyo ivanze na iyoni z'icyuma, ikungahaye ku miterere ihuza ibintu kandi ntiyoroshye kuzura. |
| Imikorere y'imirire | Ubwoko n'imikorere ya aside amine ni imwe. | Ubwoko n'imikorere ya aside amine ni imwe. | Itsindaubwoko bwinshiaside amine itanga intungamubiri yuzuye, mu gihe peptide nto zishobora gukora neza. |
| Ingaruka zo kwinjiza | Glycine chelates ifitenoAmatsinda ya karubokisili yigenga abaho kandi agira ingaruka zo kwinjiza buhoro buhoro. | Methionine chelates ifitenoAmatsinda ya karubokisili yigenga abaho kandi agira ingaruka zo kwinjiza buhoro buhoro. | Peptide chelate ntoya zakozwebirimokuba hari amatsinda ya karubokisili yigenga kandi bikagira ingaruka zo kwinjiza vuba. |
Igice cya 4 Izina ry'ubucuruzi “Peptide nto-mineral Chelates”
Chelate ntoya za Peptide-mineral, nk'uko izina ribigaragaza, biroroshye kuziba.
Bisobanura ligande nto za peptide, zidapfa kuzura bitewe n'umubare munini w'amatsinda ahuza ibintu, Byoroshye gukora chelate y'amenyo menshi hamwe n'ibintu by'icyuma, kandi ifite ubusugire bwiza.
Igice cya 5 Intangiriro ku bicuruzwa bya Peptide nto-minerale Chelates
1. Umuringa muto ugizwe n'udukoko twa peptide (izina ry'ubucuruzi: Copper Amino Acid Chelate Feed Grade)
2. Ubutare buto bw’ubutare bwa peptide (izina ry’ubucuruzi: Ferrous Amino Acid Chelate Feed Grade)
3. Uduce duto twa peptide duto kandi dufite sheleti ya zinc (izina ry'ubucuruzi: Zinc Amino Acid Chelate Feed Grade)
4. Mineral small peptide trace manganese chelated (izina ry'ubucuruzi: Manganese Amino Acid Chelate Feed Grade)
Ingano y'ibiryo bya aside amino aside chelate y'umuringa
Ingano y'ibiryo bya aside amino aside chelate ya feri
Ingano y'ibiryo bya aside ya zinki amino chelate
Ingano y'ibiryo bya Manganese Amino Acid Chelate
1. Ingano y'ibiryo bya aside amine amine y'umuringa (Copper amino acid chelate)
- Izina ry'igicuruzwa: Ingano y'ibiryo bya aside ya amino aside ya calcium Chelate
- Ishusho: Uduce tw'icyatsi kibisi cy'umukara
- Ibipimo bya fizikikemike
a) Umuringa: ≥ 10.0%
b) Aside amine yose hamwe: ≥ 20.0%
c) Igipimo cya Chelation: ≥ 95%
d) Arsenic: ≤ 2 mg/kg
e) Lead: ≤ 5 mg/kg
f) Kadiyumu: ≤ 5 mg/kg
g) Ubushuhe: ≤ 5.0%
h) Ubunini: Uduce twose duca mu mashini 20, hamwe n'uduce tw'ingenzi dufite ingano ya 60-80 mesh
n=0,1,2,... bigaragaza umuringa urimo chelate kuri dipeptides, tripeptides, na tetrapeptides
Diglycerine
Imiterere ya chelate nto ya peptide
Ibiranga uburyo ibiryo bya aside amine amine y'umuringa (Copper amino acid chelate feed grade)
- Iki gicuruzwa ni imyunyu ngugu y’ibinyabuzima byose ikomoka kuri chelating ikoresheje uburyo bwihariye bwo kuyungurura hamwe na peptides nto za enzymes z’ibimera nk’ibintu biyungurura chelating n’ibintu biyungurura
- Iki gicuruzwa ntigihinduka mu buryo busanzwe kandi gishobora kugabanya cyane kwangirika kwacyo kuri vitamine n'ibinure, nibindi.
- Gukoresha iki gicuruzwa ni byiza mu kunoza ubwiza bw'ibiryo. Iki gicuruzwa cyinjizwa mu nzira nto za peptide na aside amine, bigabanyiriza guhangana n'ibindi bintu, kandi gifite igipimo cyiza cyo kwinjiza no gukoresha ibiryo.
- Umuringa ni wo gice cy'ingenzi cy'uturemangingo dutukura tw'amaraso, ingirabuzimafatizo, amagufwa, bigira uruhare mu mubiri mu bintu bitandukanye bya enzymes, byongera imikorere y'ubudahangarwa bw'umubiri, bigabanya ingaruka za antibiyotike, bishobora kongera ibiro buri munsi, bikongera umushahara w'ibiryo.
Imikoreshereze n'Ingufu by'Uburyo bwo Kugaburira Aside Chelate ya Copper Amino Acid Chelate
| Ikintu cya porogaramu | Igipimo cyatanzwe (ibicuruzwa byuzuye bya g/t) | Ibikubiye mu ifunguro ryuzuye (mg/kg) | Ingufu |
| Kubiba | 400～700 | 60～105 | 1. Kunoza imikorere y'imyororokere n'imyaka y'ikoreshwa ry'ingurube; 2. Kongera imbaraga z'abana bato n'ingurube; 3. Kongera ubudahangarwa bw'umubiri no kurwanya indwara. |
| Icyana cy'ingurube | 300～600 | 45～90 | 1. Ifite akamaro ko kunoza imikorere y'amaraso n'ubudahangarwa bw'umubiri, kongera ubudahangarwa bw'imihangayiko no kudahangarwa n'indwara; 2. Kongera umuvuduko w'iterambere no kunoza cyane imikorere y'ibiryo by'amatungo. |
| Ingurube zibyibushye | 125 | 18.5 Mutarama | |
| Inyoni | 125 | 18.5 Mutarama | 1. Kunoza uburyo bwo kurwanya stress no kugabanya impfu; 2. Kunoza uburyo bwo kwishyura ibiryo by'amatungo no kongera umuvuduko w'izamuka ry'ingano. |
| Inyamaswa zo mu mazi | Ifi 40～70 | 6～10.5 | 1. Guteza imbere iterambere, kunoza uburyo bwo kwishyura ibiryo by'amatungo; 2. Kurwanya stress, kugabanya indwara n'impfu. |
| Isambaza 150～200 | 22.5～30 | ||
| Inyamaswa yo mu bwoko bwa g/umutwe w'inyamaswa | Mutarama 0.75 | 1. Kurinda ko ingingo zo mu gituza zihinduka, indwara yo kugenda mu mugongo, kuzungazunga, kwangirika kw'imitsi y'umutima; 2. Kurinda ko umusatsi cyangwa ikoti rihinduka keratinization, gukomera k'umusatsi, gutakaza imiterere isanzwe, gukumira "ibizinga by'imvi" mu ruziga rw'amaso; 3. Kurinda kugabanya ibiro, impiswi, umusaruro w'amata ugabanuka. |
2. Ingano y'ibiryo bya aside amine ya feri ya Chelate
- Izina ry'ibicuruzwa: Ingano y'ibiryo bya aside ya amino aside chelate ya feri
- Ishusho: Uduce tw'icyatsi kibisi cy'umukara
- Ibipimo bya fizikikemike
a) Ubutare: ≥ 10.0%
b) Aside amine yose hamwe: ≥ 19.0%
c) Igipimo cya Chelation: ≥ 95%
d) Arsenic: ≤ 2 mg/kg
e) Lead: ≤ 5 mg/kg
f) Kadiyumu: ≤ 5 mg/kg
g) Ubushuhe: ≤ 5.0%
h) Ubunini: Uduce twose duca mu mashini 20, hamwe n'uduce tw'ingenzi dufite ingano ya 60-80 mesh
n=0,1,2,...bigaragaza zinc ya chelated kuri dipeptides, tripeptides, na tetrapeptides
Ibiranga ingano y'ibiryo bya aside amine ya feri ya feri
- Iki gicuruzwa ni imyunyu ngugu y’ibinyabuzima ivangwa n’uburyo bwihariye bwo kuvura hamwe na peptides nto za enzymes z’ibimera nk’ibintu bivangwa n ...
- Iki gicuruzwa ntigihinduka mu buryo busanzwe kandi gishobora kugabanya cyane kwangirika kwacyo kuri vitamine n'ibinure, nibindi. Gukoresha iki gicuruzwa ni byiza mu kunoza ubwiza bw'ibiryo;
- Umusaruro winjizwa mu nzira nto za peptide na aside amine, bigabanya ipiganwa n'amakimbirane n'ibindi bintu, kandi bifite igipimo cyiza cyo kwinjiza no gukoresha bio-sorption;
- Uyu muti ushobora kunyura mu nzitizi ya placenta na nyababyeyi, ugatuma umwana uri mu nda agira ubuzima bwiza, wongera ibiro byo kuvuka no konka, kandi ukagabanya impfu; Ubutare ni igice cy'ingenzi cya hemoglobin na myoglobin, gishobora gukumira neza indwara yo kubura icyuma n'ingorane zacyo.
Imikoreshereze n'Ingufu by'Ingano y'Ibiryo bya Feri Amino Acid Chelate
| Ikintu cya porogaramu | Igipimo cyatanzwe (ibikoresho by'agaciro ka g/t) | Ibikubiye mu ifunguro ryuzuye (mg/kg) | Ingufu |
| Kubiba | 300～800 | 45～120 | 1. Kunoza imikorere y'imyororokere n'igihe cyo kuyikoresha; 2. kunoza ibiro by'ivuka, ibiro byo konka no guhuza ingurube kugira ngo umusaruro urusheho kuba mwiza mu gihe kiri imbere; 3. Kunoza ububiko bw'icyuma mu ngurube zonsa no gushyiramo icyuma mu mata kugira ngo hirindwe kubura amaraso mu ngurube zonsa. |
| Ibyana by'ingurube n'ingurube zibyibushye | Ibyana by'ingurube 300～600 | 45～90 | 1. Kongera ubudahangarwa bw'ingurube, kongera ubudahangarwa bw'indwara no kongera umubare w'abazima; 2. Kongera umuvuduko wo gukura, kunoza uburyo bwo guhinduranya ibiryo by'amatungo, kongera uburemere bw'ibiryo byo konka no guhuza, no kugabanya ikwirakwira ry'indwara z'ingurube; 3. Kongera urugero rwa myoglobin na myoglobin, gukumira no kuvura indwara yo kubura icyuma, gutuma uruhu rw'ingurube ruhinduka umutuku kandi birumvikana ko rutuma ibara ry'inyama rirushaho kuba ryiza. |
| Ingurube zibyibushye 200～400 | 30～60 | ||
| Inyoni | 300～400 | 45～60 | 1. Kunoza uburyo ibiryo bihinduka, kongera umuvuduko wo gukura, kongera ubushobozi bwo kurwanya stress no kugabanya impfu; 2. Kunoza umuvuduko w'amagi yo gutera, kugabanya umuvuduko w'amagi yamenetse no kongera ibara ry'umuhondo; 3. Kunoza umuvuduko wo korora no gutera amagi yororoka ndetse n'umuvuduko wo kubaho kw'inkoko nto. |
| Inyamaswa zo mu mazi | 200～300 | 30～45 | 1. Guteza imbere iterambere, kunoza ihinduka ry'ibiryo by'amatungo; 2. Kunoza uburyo bwo kurwanya stress, kugabanya indwara n'impfu. |
3. Ingano y'ibiryo bya aside ya zinki amino aside chelate
- Izina ry'igicuruzwa: Ingano y'ibiryo bya Zinc Amino Acid Chelate
- Ishusho: utunyangingo tw'umukara n'umuhondo
- Ibipimo bya fizikikemike
a) Zinc: ≥ 10.0%
b) Aside amine yose hamwe: ≥ 20.5%
c) Igipimo cya Chelation: ≥ 95%
d) Arsenic: ≤ 2 mg/kg
e) Lead: ≤ 5 mg/kg
f) Kadiyumu: ≤ 5 mg/kg
g) Ubushuhe: ≤ 5.0%
h) Ubunini: Uduce twose duca mu mashini 20, hamwe n'uduce tw'ingenzi dufite ingano ya 60-80 mesh
n=0,1,2,...bigaragaza zinc ya chelated kuri dipeptides, tripeptides, na tetrapeptides
Ibiranga uburyo Zinc Amino Acid Chelate Feed Grade
Iki gicuruzwa ni imyunyu ngugu y’ibinyabuzima byose ivangwa n’uburyo bwihariye bwo kuvura hamwe na peptides nto za enzymes z’ibimera nk’ibintu bivangwa n ...
Iki gicuruzwa ntigihinduka mu buryo busanzwe kandi gishobora kugabanya cyane kwangirika kwacyo kuri vitamine n'ibinure, nibindi.
Gukoresha iki gicuruzwa ni byiza mu kunoza ubwiza bw'ibiryo; Iki gicuruzwa cyinjizwa mu nzira nto za peptide na aside amine, bigabanyiriza ihangana n'ubushyamirane n'ibindi bintu, kandi gifite igipimo cyiza cyo kwinjiza no gukoresha ibiryo;
Iki gicuruzwa gishobora kongera ubudahangarwa bw'umubiri, guteza imbere gukura, kongera uburyo ibiryo bihindukamo no kunoza ubwiza bw'ubwoya;
Zinc ni igice cy'ingenzi cy'imisemburo irenga 200, ingirabuzimafatizo zo mu ruhu, ribose na gustatin. Itera imbere kwiyongera vuba kw'uturemangingo tw'uburyohe mu rumungu rw'ururimi kandi ikagenzura ubushake bwo kurya; ikabuza bagiteri mbi zo mu mara; kandi ifite akazi ko kuba imiti yica udukoko, ishobora kunoza imikorere y'igogora n'imikorere ya enzymes mu turemangingo.
Imikoreshereze n'Ingufu bya Zinc Amino Acid Chelate Feed Grade
| Ikintu cya porogaramu | Igipimo cyatanzwe (ibikoresho by'agaciro ka g/t) | Ibikubiye mu ifunguro ryuzuye (mg/kg) | Ingufu |
| Ingurube zitwite n'izonsa | 300～500 | 45～75 | 1. Kunoza imikorere y'imyororokere n'igihe cyo kuyikoresha; 2. Kongera imbaraga z'umwana uri mu nda n'ingurube, kongera ubudahangarwa bw'indwara, no gutuma zigira umusaruro mwiza mu gihe kiri imbere; 3. Kunoza imiterere y'umubiri w'ingurube zitwite n'uburemere bw'ingurube zivutse. |
| Ingurube y'ingore, ingurube y'ingore n'ingurube zibyibushye | 250～400 | 37.5～60 | 1. Kongera ubudahangarwa bw'ingurube, kugabanya impiswi n'impfu; 2. Kunoza uburyo ibiryo biryoha, kongera uburyo ibiryo bihabwa, kongera umuvuduko wo gukura no kunoza uburyo ibiryo bihindukamo; 3. Ongera ubwiza bw'ingurube no kunoza ubwiza bw'inka n'ubwiza bw'inyama. |
| Inyoni | 300～400 | 45～60 | 1. Kunoza ubwiza bw'ubwoya; 2. kunoza uburyo amagi yororoka, uburyo atera, n'uburyo yororoka, no kongera ubushobozi bwo gusiga ibara ry'umuhondo w'igi; 3. Kunoza ubushobozi bwo kurwanya stress no kugabanya impfu; 4. Kunoza ihinduka ry'ibiryo by'amatungo no kongera umuvuduko wo gukura. |
| Inyamaswa zo mu mazi | Mutarama 300 | 45 | 1. Guteza imbere iterambere, kunoza ihinduka ry'ibiryo by'amatungo; 2. Kunoza uburyo bwo kurwanya stress, kugabanya indwara n'impfu. |
| Inyamaswa yo mu bwoko bwa g/umutwe w'inyamaswa | 2.4 | 1. Kongera umusaruro w'amata, hirindwa mastite no kubora kw'ibinono, kandi bigabanye ingano y'uturemangingo tw'amata mu mata; 2. Guteza imbere iterambere, kunoza ihinduka ry'ibiryo by'amatungo no kunoza ubwiza bw'inyama. |
4. Ingano y'ibiryo bya Manganese Amino Acide Chelate
- Izina ry'ibicuruzwa: Ingano y'ibiryo bya Manganese Amino Acid Chelate
- Ishusho: utunyangingo tw'umukara n'umuhondo
- Ibipimo bya fizikikemike
a) Mn: ≥ 10.0%
b) Aside amine yose hamwe: ≥ 19.5%
c) Igipimo cya Chelation: ≥ 95%
d) Arsenic: ≤ 2 mg/kg
e) Lead: ≤ 5 mg/kg
f) Kadiyumu: ≤ 5 mg/kg
g) Ubushuhe: ≤ 5.0%
h) Ubunini: Uduce twose duca mu mashini 20, hamwe n'uduce tw'ingenzi dufite ingano ya 60-80 mesh
n=0, 1,2,...bigaragaza manganese ya chelated kuri dipeptides, tripeptides, na tetrapeptides
Ibiranga uburyo Manganese Amino Acid Chelate Feed Grade
Iki gicuruzwa ni imyunyu ngugu y’ibinyabuzima byose ivangwa n’uburyo bwihariye bwo kuvura hamwe na peptides nto za enzymes z’ibimera nk’ibintu bivangwa n ...
Iki gicuruzwa ntigihinduka mu buryo busanzwe kandi gishobora kugabanya cyane kwangirika kwacyo kuri vitamine n'ibinure, nibindi. Gukoresha iki gicuruzwa ni byiza mu kunoza ubwiza bw'ibiryo;
Umusaruro winjizwa mu nzira nto za peptide na aside amine, bigabanya ipiganwa n'amakimbirane n'ibindi bintu, kandi bifite igipimo cyiza cyo kwinjiza no gukoresha bio-sorption;
Ibi bicuruzwa bishobora kongera umuvuduko wo gukura, kongera uburyo ibiryo bihinduka n'ubuzima bw'inkoko mu buryo bugaragara; no kongera umuvuduko wo gutera, gutera imbuto no kororoka kw'inkoko mu buryo bufatika;
Manganese ni ngombwa mu gukura kw'amagufwa no kubungabunga ingirabuzimafatizo. Ifitanye isano rya hafi na enzymes nyinshi; kandi igira uruhare mu mikorere ya karubohidrati, ibinure na poroteyine, kororoka no gukora neza kw'ubudahangarwa bw'umubiri.
Imikoreshereze n'Ingufu bya Manganese Amino Acid Chelate Feed Grade
| Ikintu cya porogaramu | Igipimo cyatanzwe (ibicuruzwa byuzuye bya g/t) | Ibikubiye mu ifunguro ryuzuye (mg/kg) | Ingufu |
| Ingurube yororerwa | 200～300 | 30～45 | 1. Guteza imbere imikurire isanzwe y'imyanya ndangagitsina no kunoza uburyo intanga zigenda; 2. Kongera ubushobozi bwo kororoka bw'ingurube no kugabanya imbogamizi zo kororoka. |
| Ibyana by'ingurube n'ingurube zibyibushye | 100～250 | 15～37.5 | 1. Ni ingirakamaro mu kunoza imikorere y'ubudahangarwa bw'umubiri, no kunoza ubushobozi bwo kurwanya stress no kurwanya indwara; 2. Guteza imbere iterambere no kunoza uburyo ibiryo bihindukamo cyane; 3. Kongera ibara ry'inyama n'ubwiza bwazo, no kongera igipimo cy'inyama zitarimo ibinure. |
| Inyoni | 250～350 | 37.5～52.5 | 1. Kunoza ubushobozi bwo kurwanya stress no kugabanya impfu; 2. Kunoza uburyo amagi yororoka, uburyo atera intanga n'uburyo yororoka, kunoza ubwiza bw'ibishyimbo by'amagi no kugabanya uburyo amagi yororoka; 3. Guteza imbere gukura kw'amagufwa no kugabanya indwara z'amaguru. |
| Inyamaswa zo mu mazi | 100～200 | 15～30 | 1. Guteza imbere iterambere no kunoza ubushobozi bwayo bwo kurwanya stress no kurwanya indwara; 2. Kongera ubushobozi bwo kugenda kw'intanga no gusohora amagi y'intanga. |
| Inyamaswa yo mu bwoko bwa g/umutwe w'inyamaswa | Inka 1.25 | 1. Kurinda indwara yo gukora aside irike no kwangirika kw'imitsi y'amagufwa; 2. Kongera ubushobozi bwo kororoka, gukumira gukuramo inda no gucika intege kw'amatungo y'ingore nyuma yo kubyara, kugabanya urupfu rw'inyana n'intama, no kongera ibiro by'amatungo magufi avutse. | |
| Ihene 0.25 |
Igice cya 6 FAB ya Peptide nto-mineral Chelates
| S/N | F: Imiterere y'imikorere | A: Itandukaniro mu marushanwa | B: Inyungu zizanwa n'itandukaniro ry'irushanwa ku bakoresha |
| 1 | Kugenzura uburyo ibikoresho fatizo bitoranywa | Hitamo hydrolysis y'ibimera byuzuye ya peptide nto | Umutekano mwinshi w’ibinyabuzima, birinda kurya abantu |
| 2 | Ikoranabuhanga ryo gusya poroteyine ebyiri mu buryo buyobora enzyme y'ibinyabuzima | Igice kinini cya peptide nto za molekile | "Intego" nyinshi, zitari zoroshye kuzishyira ku rugero rumwe, zifite imikorere myinshi y'ibinyabuzima kandi zikagira umutekano mwiza |
| 3 | Ikoranabuhanga rigezweho ryo gusukura no kumisha | Igicuruzwa cy'ibinyabutabire, gifite ingano imwe y'uduce, gifite amazi menshi, nticyoroshye kwinjiza amazi | Menya neza ko byoroshye gukoresha, kandi bivanze neza mu buryo bumwe mu buryo bwuzuye |
| Amazi make (≤ 5%), bigabanya cyane ingaruka ziterwa na vitamine n'imisemburo | Kunoza uburyo ibicuruzwa bitunganywa mu buryo buhamye | ||
| 4 | Ikoranabuhanga rigezweho ryo kugenzura umusaruro | Uburyo bufunze neza, urwego rwo hejuru rw'igenzura ryikora | Ubwiza butekanye kandi buhamye |
| 5 | Ikoranabuhanga rigezweho ryo kugenzura ubuziranenge | Gushyiraho no kunoza uburyo bwa siyansi n'ubuhanga bwo gusesengura hamwe n'uburyo bwo kugenzura ibintu bigira ingaruka ku bwiza bw'umusaruro, nka poroteyine ishonga na aside, ikwirakwizwa ry'uburemere bwa molekile, aside amine n'igipimo cya chelating. | Kugenzura ubuziranenge, kugenzura imikorere myiza no kunoza imikorere myiza |
Igice cya 7 cyo kugereranya abarushanwa
Igipimo ngenderwaho cya VS
Kugereranya ikwirakwizwa rya peptide n'igipimo cya chelation y'ibicuruzwa
| Ibicuruzwa bya Sustar | Ingano ya peptide nto (180-500) | Ibicuruzwa bya Zinpro | Ingano ya peptide nto (180-500) |
| AA-Cu | ≥74% | AVAILA-Cu | 78% |
| AA-Fe | ≥48% | AVAILA-Fe | 59% |
| AA-Mn | ≥33% | AVAILA-Mn | 53% |
| AA-Zn | ≥37% | AVAILA-Zn | 56% |
| Ibicuruzwa bya Sustar | Igipimo cya Chelation | Ibicuruzwa bya Zinpro | Igipimo cya Chelation |
| AA-Cu | 94.8% | AVAILA-Cu | 94.8% |
| AA-Fe | 95.3% | AVAILA-Fe | 93.5% |
| AA-Mn | 94.6% | AVAILA-Mn | 94.6% |
| AA-Zn | 97.7% | AVAILA-Zn | 90.6% |
Igipimo cya peptide nto za Sustar kiri hasi gato ugereranyije n’icya Zinpro, kandi igipimo cya chelation cy’ibicuruzwa bya Sustar kiri hejuru gato ugereranyije n’ibicuruzwa bya Zinpro.
Kugereranya ibikubiye muri aside amine 17 mu bicuruzwa bitandukanye
| Izina rya aside amine | Umuringa wa Sustar Chelate ya aside amine Icyiciro cyo kugaburira | Zinpro's BIRABONEKA umuringa | Aside amino ya Sustar yitwa Ferrous Amino C Hellate Feed Icyiciro | Zinpro's ABONETSE icyuma | Manganese ya Sustar Chelate ya aside amine Icyiciro cyo kugaburira | Zinpro's ABONETSE manganese | Sustar's Zinc aside amine Ingano y'ibiryo bya Chelate | Zinpro's ABONETSE zinki |
| aside aspartike (%) | 1.88 | 0.72 | 1.50 | 0.56 | 1.78 | 1.47 | 1.80 | 2.09 |
| aside glutamike (%) | 4.08 | 6.03 | 4.23 | 5.52 | 4.22 | 5.01 | 4.35 | 3.19 |
| Serine (%) | 0.86 | 0.41 | 1.08 | 0.19 | 1.05 | 0.91 | 1.03 | 2.81 |
| Histidine (%) | 0.56 | 0.00 | 0.68 | 0.13 | 0.64 | 0.42 | 0.61 | 0.00 |
| Glycine (%) | 1.96 | 4.07 | 1.34 | 2.49 | 1.21 | 0.55 | 1.32 | 2.69 |
| Threonine (%) | 0.81 | 0.00 | 1.16 | 0.00 | 0.88 | 0.59 | 1.24 | 1.11 |
| Arginine (%) | 1.05 | 0.78 | 1.05 | 0.29 | 1.43 | 0.54 | 1.20 | 1.89 |
| Alanine (%) | 2.85 | 1.52 | 2.33 | 0.93 | 2.40 | 1.74 | 2.42 | 1.68 |
| Tyrosinase (%) | 0.45 | 0.29 | 0.47 | 0.28 | 0.58 | 0.65 | 0.60 | 0.66 |
| Cystinol (%) | 0.00 | 0.00 | 0.09 | 0.00 | 0.11 | 0.00 | 0.09 | 0.00 |
| Valine (%) | 1.45 | 1.14 | 1.31 | 0.42 | 1.20 | 1.03 | 1.32 | 2.62 |
| Methionine (%) | 0.35 | 0.27 | 0.72 | 0.65 | 0.67 | 0.43 | Mutarama 0.75 | 0.44 |
| Phenylalanine (%) | 0.79 | 0.41 | 0.82 | 0.56 | 0.70 | 1.22 | 0.86 | 1.37 |
| Isoleusine (%) | 0.87 | 0.55 | 0.83 | 0.33 | 0.86 | 0.83 | 0.87 | 1.32 |
| Leusini (%) | 2.16 | 0.90 | 2.00 | 1.43 | 1.84 | 3.29 | 2.19 | 2.20 |
| Lisine (%) | 0.67 | 2.67 | 0.62 | 1.65 | 0.81 | 0.29 | 0.79 | 0.62 |
| Proline (%) | 2.43 | 1.65 | 1.98 | 0.73 | 1.88 | 1.81 | 2.43 | 2.78 |
| Aside amine yose (%) | 23.2 | 21.4 | 22.2 | 16.1 | 22.3 | 20.8 | 23.9 | 27.5 |
Muri rusange, igipimo cya aside amine mu bicuruzwa bya Sustar kiri hejuru kurusha icyo mu bicuruzwa bya Zinpro.
Igice cya 8 Ingaruka zo gukoresha
Ingaruka z'amasoko atandukanye y'imyunyu ngugu ku musaruro n'ubwiza bw'amagi y'inkoko zitera mu gihe cyo gutera amagi mu mpera z'igihe cyo gutera amagi
Uburyo bwo gukora
- Ikoranabuhanga rya chelation rigamije
- Ikoranabuhanga ryo gukata ibyuma bivanze n'amazi
- Ikoranabuhanga ryo gusukura no kumisha umuvuduko
- Ikoranabuhanga ryo gushyira muri firigo no gukuraho ubushuhe
- Ikoranabuhanga rigezweho ryo kugenzura ibidukikije
Umugereka A: Uburyo bwo kumenya ikwirakwizwa ry'uburemere bwa molekile bwa peptides
Kwemeza ibipimo ngenderwaho: GB/T 22492-2008
1 Ihame ry'ikizamini:
Byagenwe hakoreshejwe chromatography ya gel filtration ifite ubushobozi bwo hejuru. Ni ukuvuga, hakoreshejwe uburyo bwo gupima imyenge nk'ikiciro gihoraho, hashingiwe ku itandukaniro riri hagati y'ingano y'uburemere bwa molekile bw'ibice by'icyitegererezo kugira ngo bitandukanywe, byagaragaye ku mugozi wa peptide w'uburebure bwa ultraviolet bwo kwinjiza 220nm, hakoreshejwe porogaramu yihariye yo gutunganya amakuru kugira ngo hamenyekane ikwirakwizwa ry'uburemere bwa molekile hakoreshejwe chromatography ya gel filtration (ni ukuvuga porogaramu ya GPC), chromatograms n'amakuru yazo byaratunganyijwe, bibarwa kugira ngo hamenyekane ingano y'uburemere bwa molekile bwa peptide ya soya n'urwego rw'ikwirakwizwa.
2. Ibikoresho bitanga umusaruro
Amazi yo mu igerageza agomba kuba yujuje ibisabwa n'amazi y'inyongera muri GB/T6682, ikoreshwa ry'ibisubizo, uretse ingingo zihariye, ni nta busesenguzi.
2.1 Ibintu bigabanya ubukana birimo acetonitrile (icyiza mu buryo bwa chromatographic), aside trifluoroacetic (icyiza mu buryo bwa chromatographic),
2.2 Ibintu bisanzwe bikoreshwa mu gupima ikwirakwizwa ry'uburemere bwa molekile: insuline, mycopeptides, glycine-glycine-tyrosine-arginine, glycine-glycine-glycine
3 Ibikoresho n'ibikoresho
3.1 Chromatograph y'amazi ifite imikorere myiza (HPLC): ikigo cy'ikoranabuhanga cya chromatographic cyangwa integrator gifite icyuma gipima UV na porogaramu yo gutunganya amakuru ya GPC.
3.2 Igice cyo kuyungurura no gukuramo imyuka mu buryo bugendanwa.
3.3 Amafaranga asigaye mu buryo bw'ikoranabuhanga: agaciro kagabanijwe 0.000 1g.
Intambwe 4 z'imikorere
4.1 Imiterere ya kromatografiya n'igerageza ryo guhuza sisitemu (imiterere y'icyitegererezo)
4.1.1 Inkingi ya kromatografiya: TSKgelG2000swxl300 mm×7.8 mm (umurambararo w'imbere) cyangwa izindi nkingi za jeli z'ubwoko bumwe zifite imikorere isa ikwiriye mu kugena poroteyine na peptides.
4.1.2 Icyiciro cyo kugenda: Acetonitrile + amazi + aside trifluoroacetic = 20 + 80 + 0.1.
4.1.3 Uburebure bw'urumuri rupima: 220 nm.
4.1.4 Igipimo cy'amazi atemba: 0.5 mL/umunota.
4.1.5 Igihe cyo gutahura: iminota 30.
4.1.6 Ingano y'icyitegererezo cy'urushinge: 20μL.
4.1.7 Ubushyuhe bw'inkingi: ubushyuhe bw'icyumba.
4.1.8 Kugira ngo sisitemu ya chromatografiya yuzuze ibisabwa mu gupima, byagenwe ko hakurikijwe imiterere ya chromatografiya yavuzwe haruguru, imikorere ya gel chromatografiya, ni ukuvuga umubare w’amapine (N), itari munsi ya 10000 yabazwe hashingiwe ku ntera z’ibipimo bya tripeptide (Glycine-Glycine-Glycine).
4.2 Gukora imigozi isanzwe y'uburemere bwa molekile
Ibisubizo bitandukanye byavuzwe haruguru bya peptide isanzwe ifite uburemere bwa 1 mg / mL byateguwe hakoreshejwe uburyo bwo guhuza imiterere y’ibice, bivangwa mu rugero runaka, hanyuma bigasukurwa binyuze mu ruhu rw’imiterere y’ibice bifite ingano ya 0.2 μm ~ 0.5 μm hanyuma bigashyirwa mu gipimo, hanyuma haboneka chromatogramu z’ibipimo. Imirongo yo gupima uburemere bwa molekile n’ibipimo byabyo byabonetse hakoreshejwe uburyo bwo gushushanya logarithm y’ubunini bwa molekile hakurikijwe igihe cyo kubigumana cyangwa hakoreshejwe umurongo ugororotse.
4.3 Icyitegererezo cy'uburyo bwo kuvura
Pima neza 10mg y'icyitegererezo mu icupa rya 10ml volumetric, ongeramo agace gato kagendanwa, ugatengure ultrasonic mu gihe cy'iminota 10, kugira ngo icyitegererezo gishonge neza kandi kivangwe, givangwe na mobile phase kugeza ku gipimo, hanyuma kinyurwe mu ruhu rw'ingirabuzimafatizo rufite imyenge ya 0.2μm ~ 0.5μm, hanyuma filtrate isesengurwe hakurikijwe imiterere ya chromatographic muri A.4.1.
5. Kubara ikwirakwizwa ry'uburemere bwa molekile
Nyuma yo gusesengura igisubizo cy'icyitegererezo cyateguwe muri 4.3 hakurikijwe imiterere ya kromatografiya ya 4.1, uburemere bwa molekile y'icyitegererezo n'urwego rwacyo rukwirakwizwa bishobora kuboneka hakoreshejwe uburyo bwa kromatografiya bw'icyitegererezo mu buryo bwa calibration 4.2 na porogaramu ya GPC yo gutunganya amakuru. Ikwirakwizwa ry'ubunini bwa molekile y'ama peptide atandukanye rishobora kubarwa hakoreshejwe uburyo bwo kugena ahantu hanini, hakurikijwe formula: X=A/A igiteranyo ×100
Muri formula: X - Igice cy'uburemere bwa peptide y'uburemere bwa molekile muri peptide yose mu gipimo, %;
A - Agace k'impinga ya peptide y'umubare wa molekile;
Igiteranyo A - igiteranyo cy'ubuso bw'impinga ya buri peptide y'ubunini bwa molekile, ibarwa kugeza ahantu hamwe ho kugabanya.
6 Gusubiramo
Itandukaniro rigaragara hagati y’ibizamini bibiri byigenga byabonetse mu buryo bwo gusubiramo ntibigomba kurenga 15% by’ikigereranyo cy’imibare cy’ibyavuye mu bizamini byombi.
Umugereka B: Uburyo bwo kumenya aside amine zidafite amino
Kwemeza ibipimo ngenderwaho: Q/320205 KAVN05-2016
1.2 Ibikoresho bitanga umusaruro n'ibikoresho
Aside asetiki y'ibara rya glacial: isukuye mu buryo bw'isesengura
Aside ya perchloric: 0.0500 mol/L
Ikimenyetso: Ikimenyetso cya 0.1% cya kristalo violet (aside acetic glacial)
2. Kumenya aside amine zifunguye
Ingero zarumishijwe kuri dogere selisiyusi 80 mu gihe cy'isaha imwe.
Shyira icyitegererezo mu kintu cyumye kugira ngo gikonje mu buryo busanzwe kugeza ku bushyuhe bw'icyumba cyangwa gikonje kugeza ku bushyuhe bushoboka.
Pima hafi garama 0.1 z'icyitegererezo (kimeze neza kugeza kuri garama 0.001) mu icupa ryumye rya mL 250.
Komeza vuba intambwe ikurikiraho kugira ngo wirinde ko icyitegererezo cyakwinjirira ubushuhe bwo mu kirere
Ongeraho mililitiro 25 za aside asetiki y'urubura hanyuma uvange neza mu gihe kitarenze iminota 5.
Ongeraho ibitonyanga 2 by'ikimenyetso cya crystal violet
Titrate hamwe na 0.0500 mol / L (± 0.001) igisubizo gisanzwe cya titration cya aside perchloric kugeza igihe igisubizo gihindutse kuva ku ibara ry'umuhengeri kugera ku iherezo.
Andika ingano y'umuti usanzwe wakoreshejwe.
Kora ikizamini cy'ubusa icyarimwe.
3. Kubara n'ibisubizo
Ingano ya aside amine X iri muri reagent igaragazwa nk'igice cy'uburemere (%) kandi ibarwa hakurikijwe formula: X = C × (V1-V0) × 0.1445/M × 100%, muri formula ya tne:
C - Ingano y'umuti usanzwe wa aside perchloric muri moles kuri litiro (mol/L)
V1 - Ingano ikoreshwa mu gupima ingero hakoreshejwe umuti usanzwe wa aside perchloric, muri mililitiro (mL).
Vo - Ingano ikoreshwa mu gupima ubusa hamwe n'umuti usanzwe wa aside perchloric, muri mililitiro (mL);
M - Uburemere bw'icyitegererezo, muri garama (g).
0.1445: Uburemere bw'impuzandengo ya aside amine bungana na mL 1.00 z'umuti usanzwe wa aside perchloric [c (HClO4) = 1.000 mol / L].
Umugereka C: Uburyo bwo kumenya igipimo cya Sustar cyo gupima
Kwemeza amahame ngenderwaho: Q/70920556 71-2024
1. Ihame ryo guhitamo (urugero rwa Fe)
Ibyuma bya aside amino bifite ubushobozi buke bwo gushonga muri ethanol idafite amazi kandi iyoni z’icyuma zishongesha muri ethanol idafite amazi, itandukaniro mu gushonga hagati yabyo bibiri muri ethanol idafite amazi ryakoreshejwe kugira ngo hamenyekane igipimo cya chelation cy’ibice bya aside amino ibyuma.
2. Ibikoresho bitanga umusaruro n'ibisubizo
Ethanol idakoresha amazi; ibisigaye ni kimwe n'ingingo ya 4.5.2 muri GB/T 27983-2011.
3. Intambwe zo gusesengura
Kora igerageza ribiri icyarimwe. Pima garama 0.1 z'icyitegererezo cyumye kuri dogere 103±2℃ mu gihe cy'isaha 1, neza kuri garama 0.0001, ongeramo garama 100 za etanoli idafite amazi kugira ngo ishonge, yungurura, yungurura ibisigazwa byogejwe na garama 100 za etanoli idafite amazi nibura inshuro eshatu, hanyuma ushyire ibisigazwa mu icupa rya garama 250, ongeramo garama 10 z'umuti wa aside sulfure nk'uko bivugwa mu ngingo ya 4.5.3 muri GB/T27983-2011, hanyuma ukore ibi bikurikira nk'uko bivugwa mu ngingo ya 4.5.3 "Shusha kugira ngo ishonge hanyuma uyireke ikonje" muri GB/T27983-2011. Kora ikizamini cy'ubusa icyarimwe.
4. Kumenya ingano y'icyuma cyose
4.1 Ihame ryo kugena ni kimwe n'ingingo ya 4.4.1 muri GB/T 21996-2008.
4.2. Ibikoresho bitanga umusaruro n'ibisubizo
4.2.1 Aside ivanze: Shyira mililitiro 150 za aside sulfurike na mililitiro 150 za aside phosphorike muri mililitiro 700 z'amazi hanyuma uvange neza.
4.2.2 Umuti w'ikimenyetso cya Sodium diphenylamine sulfonate: 5g/L, wateguwe hakurikijwe GB/T603.
4.2.3 Umuti usanzwe wa Cerium sulfate: igipimo c [Ce (SO4) 2] = 0.1 mol/L, wateguwe hakurikijwe GB/T601.
4.3 Intambwe zo gusesengura
Kora igerageza ribiri icyarimwe. Pima garama 0.1 z'icyitegererezo, gihuye na garama 020001, shyira mu icupa rya mililitiro 250, ongeramo mililitiro 10 z'aside ivanze, nyuma yo gushonga, ongeramo mililitiro 30 z'amazi n'ibitonyanga 4 bya sodium dianiline sulfonate, hanyuma ukore ibi bikurikira nk'uko bivugwa mu ngingo ya 4.4.2 muri GB/T21996-2008. Kora ikizamini cy'ubusa icyarimwe.
4.4 Igaragazwa ry'ibyavuye mu bushakashatsi
Igiteranyo cy'icyuma X1 cy'ibice by'icyuma bya aside amine mu buryo bw'igice cy'icyuma, agaciro kagaragazwa muri %, kabazwe hakurikijwe formula (1):
X1 = (V-V0) × C × M × 10-3 × 100
Muri formula: V - ingano y'umuti usanzwe wa cerium sulfate ukoreshwa mu gupima umuti, mL;
V0 - umuti usanzwe wa cerium sulfate ukoreshwa mu gupima umuti udafite ikintu, mL;
C - Igipimo nyacyo cy'umuti usanzwe wa cerium sulfate, mol/L
5. Kubara ingano y'icyuma muri chelate
Ingano y'icyuma X2 muri chelate hakurikijwe igice cy'uburemere bw'icyuma, agaciro kagaragazwa muri %, kabazwe hakurikijwe formula: x2 = ((V1-V2) × C × 0.05585)/m1 × 100
Muri formula: V1 - ingano y'umuti usanzwe wa cerium sulfate ukoreshwa mu gupima umuti, mL;
V2 - umuti usanzwe wa cerium sulfate ukoreshwa mu gupima umuti udafite ikintu, mL;
C - Igipimo nyacyo cy'umuti usanzwe wa cerium sulfate, mol/L;
0.05585 - uburemere bw'icyuma cya ferrous cyagaragaye muri garama zingana na 1.00 mL y'umuti usanzwe wa cerium sulfate C[Ce(SO4)2.4H20] = 1.000 mol/L.
m1 - Uburemere bw'icyitegererezo, g. Fata impuzandengo y'imibare y'ibyavuye mu gupima parallel nk'ibisubizo by'igenamigambi, kandi itandukaniro risesuye ry'ibyavuye mu gupima parallel ntirirenze 0.3%.
6. Kubara igipimo cya chelation
Igipimo cya Chelation X3, agaciro kagaragajwe muri %, X3 = X2/X1 × 100
Umugereka C: Uburyo bwo kumenya igipimo cya Zinpro cyo gupima ingano y'amaraso
Kwemeza ibipimo ngenderwaho: Q/320205 KAVNO7-2016
1. Ibikoresho bitanga umusaruro n'ibikoresho
a) Aside acetike y'ibara rya glacial: isukuye mu buryo bw'isesengura; b) Aside ya perchloric: 0.0500mol/L; c) Ikimenyetso: Ikimenyetso cya 0.1% cya crystal violet (aside acetike y'ibara rya glacial)
2. Kumenya aside amine zifunguye
2.1 Ingero zarumishijwe kuri dogere selisiyusi 80 mu gihe cy'isaha imwe.
2.2 Shyira icyitegererezo mu kintu cyumye kugira ngo gikonje mu buryo busanzwe kugeza ku bushyuhe bw'icyumba cyangwa gikonje kugeza ku bushyuhe bushoboka.
2.3 Pima hafi garama 0.1 z'icyitegererezo (kimeze neza kugeza kuri garama 0.001) mu icupa ryumye rya mL 250
2.4 Subiramo vuba intambwe ikurikira kugira ngo wirinde ko icyitegererezo cyakwinjirira ubushuhe bwo mu kirere.
2.5 Ongeramo 25ml ya aside asetiki y'urubura hanyuma uvange neza mu gihe kitarenze iminota 5.
2.6 Ongeraho ibitonyanga 2 by'ikimenyetso cya crystal violet.
2.7 Titrate hamwe na 0.0500mol/L (±0.001) umuti usanzwe wa titration wa aside perchloric kugeza igihe umuti uhindutse kuva ku ibara ry'umuhengeri ukajya ku ibara ry'icyatsi mu gihe cy'iminota 15 nta guhindura ibara nk'aho ari iherezo.
2.8 Andika ingano y'umuti usanzwe wakoreshejwe.
2.9 Kora ikizamini cy'ubusa icyarimwe.
3. Kubara n'ibisubizo
Ingano ya aside amine X iri muri reagent igaragazwa nk'igice cy'uburemere (%), ibarwa hakurikijwe formula (1): X=C×(V1-V0) ×0.1445/M×100%.......(1)
Muri formula: C - ingano y'umuti usanzwe wa aside perchloric muri moles kuri litiro (mol/L)
V1 - Ingano ikoreshwa mu gupima ingero hakoreshejwe umuti usanzwe wa aside perchloric, muri mililitiro (mL).
Vo - Ingano ikoreshwa mu gupima ubusa hamwe n'umuti usanzwe wa aside perchloric, muri mililitiro (mL);
M - Uburemere bw'icyitegererezo, muri garama (g).
0.1445 - Uburemere bw'impuzandengo ya aside amine bungana na mL 1.00 z'umuti usanzwe wa aside perchloric [c (HClO4) = 1.000 mol / L].
4. Kubara igipimo cya chelation
Igipimo cya chelation cy'icyitegererezo kigaragazwa nk'igice cy'uburemere (%), kibarwa hakurikijwe formula (2): igipimo cya chelation = (ibikubiye muri aside amine yose - ibikubiye muri aside amine yigenga) / ibikubiye muri aside amine yose × 100%.
Igihe cyo kohereza: 17 Nzeri 2025
